Exploring the Role of Vial Inserts in Minimizing Sample Carryover

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in a beaker. With all of the sample introduction lines hooked up, move the autosampler probe into 50 ml vials of each of the following solutions: • ~30% NH 4OH (30 min with peri at 0.3 rps) • ~30% HCl (30 min with peri at 0.3 rps) • ~30% HNO 3 (30 min with peri at 0.3 rps) • De-ionized (a few minutes at 0.3 rps)

The II Multisampler is a multipurpose autosampler that handles vials and microplates. Injecting at pressures up to 1300 bar, the Multisampler is a compact module with a capacity of up to 6,144 samples, all within the footprint of an Aijiren LC stack. The II Multisampler is optimized for highest chromatographic

Glass Insert, 250 µL Volume, 100/pk. To offer ideal needle conditions when sample volume is limited, it’s important to use a Glass Insert in your sample collection vial. This glass insert, available in a pack of 100, offers 250 µL in volume and it sits securely within your vial. To operate properly, you also need a glass insert spring (PN

Sample/Standard Carryover. I am running GC (FID detector) alongside headspace. I had noticed 4 of my later eluting peaks got increasingly worse in terms of shape and reproducibility. After running blanks (no injection and also blank vials), it seemed like the cause of this turns out to be carryover.

The current venue of HPLC’s (or UHPLC’s) have vendor specific approaches to combating carryover. If we look at the Shimadzu Nexera X2 UHPLC system, we have the ability to wash just about everything our sample or standards meet within the injection system. You can dip and back-flush the exterior of the needle or rinse the inside of it too.

Vial cap leak Use new sample Reseal vial Leaking inlet septum Replace/tighten septum Leaking connections Inspect and reseal connections Split flow too high Reduce split/GC flow Sample contamination Seal immediately Minimize transfer times Ambient air contaminants Purge vial with argon before sealing Sample carryover Clean sampling needle Sample

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parameters to minimize carryover in any application. Autosampler-related carryover can occur at the inside or outside surfaces of the needle, the needle seat, and the injection valve. The following functions of the Multisampler can be used to minimize carryover: • Internal needle wash • External needle wash • Needle seat backfl ush

Jul 31, 2020 · 1. Increased Precision and Accuracy. HPLC inserts feature precise designs and dimensions to provide accurate and reproducible results, while micro vial inserts minimize sample loss during injection for precise quantitative analysis. Their tight-fitting nature means minimal sample loss during injection and ensures all sample volume reaches the

One statement that you made which concerns me is: "For example, if I have 83 µl in my microvolume insert and it is doing 80 µl injections, some of the vials are nearly empty after analysis (that

- A setpoint of -2 mm will sample 1.6 mm from the vial bottom - Range is -2 mm to 30 mm • Example uses: - Samples with sediment (although properly filtering the sample is ideal) - Sampling from higher in the sample vial in liquid-liquid extractions - Small volume sampling • Exercise caution when using sample offsets in combination with vial

9 mm Fused Insert Vial Clear Yes 12 x 32 Insert Vial 475 µL 350 µL <2 10781-890 100 – 9 mm Fused Insert Vial Amber No 12 x 32 Insert Vial 475 µL 350 µL <2 10803-888 100 – 300 µL Spring Insert Clear – 6 x 31 Conical 375 µL 250 µL <1 46610-762 100 – Polypropylene – 6 x 30 Conical 325 µL 250 µL <2 100 –

Jun 20, 2023 · Carryover, or sample contamination from previous injections, can significantly impact the accuracy and reliability of HPLC results. Micro vial inserts play a crucial role in minimizing carryover effects by providing a barrier between samples.

Crimp-Top Verex™ vials use cost-effective aluminum crimp seals. When properly assembled, this vial-cap combination provides the best seal for long term sample storage, as well as high volatility solvents. 12 x 32 mm, 11 mm Crimp-Top Vials and Closures Crimp-Top Vials, 2.0 mL • Cleaner vials eliminate ghost peaks and contaminants