Exploring the Impact of Vial Dimension on Injection Precision in Autosamplers

To validate autosampler accuracy, install a tared vial and inject a volume that is conveniently verified gravimetrically. For manual injections, if pea ks are too small, check the needle port for leaks. Peaks Too Large The autosampler is not likely to be the cause of peaks that are too large, unless the metering heads are the incorrect size.

High precision, reliability, ruggedness, and ease of use; automates many bench-top tasks; can be used with entire ICS product family. A low-cost, metal-free, rugged, automated sample loading solution with random access and sample preparation capabilities. High sample volumes up to 250 mL; AutoPrep option for trace analysis; compact footprint.

prep FAST X are advanced inline dilution systems designed for ICP & ICPMS. They unite the intelligent autocorrection capabilities of DXCi autosamplers and the automated rapid throughput of SampleSense FAST valves with a precision syringe module to perform precise and accurate inline dilutions of standards.

Aug 1, 2019 · This installment is the second of a series of four white papers on high-performance liquid chromatography (HPLC) modules focusing on pumps, autosamplers, ultraviolet (UV) detectors, and

Monowave 450 is a modern microwave reactor specially designed for microwave-assisted extractions in analytical laboratories. Its 24-position autosampler MAS24 for 30 mL Wide-Neck vials provides unattended reliable operation and increases the sample throughput. Injection Style: Vial; Capacity: 20 Number of Vials: 24 User Interface: Digital

Combing excellent injection precision with extra-large sample capacity, Thermo Scientific Vanquish autosamplers deliver superior confidence in peak identification and quantitation, and unsurpassed sample precision. An available dual split sampler is designed for use with the Thermo Scientific Vanquish Duo UHPLC system for Dual LC workflows.

a vial septum and then installing the vial in the sample tray. I adjust the needle to the target depth, then lift the vial by its cap. In the case of my instrument, I expect approximately 1 mm of vertical play if the system is adjusted properly. This play allows a safety margin in case of any variation in vial depth for a given vial model. This

full-size rack holds 100 × 1.8 mL vials, while the two half-size racks provide space for 40 × 1.8 mL vials and 15 × 6 mL vials respectively. Any two half-size rack trays can be installed in the autosampler simultaneously. A specially designed sample-rack holding 100 × 1.8 mL vials is available for use with thermostatted autosamplers.

Sep 11, 2023 · Variable sample injection volume and total volume direct injection: Injection Volume Range: 0.1 µL to 100 µL (0.1 µL to 2000 µL with option) Number of Samples Processed: 175 (1-mL vials), 105 (1.5-mL vials), 50 (4-mL vials), 192 (two 96-well MTP/DWP), 768 (two 384-well MTP/DWP) *Twelve 96-well MTP/DWP in the rackchanger: Injection Volume

High Precision and Endurance. High precision is maintained even at small injection volumes (RSD less than 1% at 1 µL injection). A minute injection of 100 nL is also possible. The standard sampling volume ranges from 0.1 to 80.0 µL. *Up to 400 µL injection can be made by using multiple collection injection.

Sep 26, 2018 · All this is possible without human intervention. Such high precision injections are not possible if repeat injections are carried out manually. Vial selection. The autosampler tray has numbered slots for positioning of sample vials. The autosampler is pre-programmed to select the vials in the desired sequence for making injections.

• Autosamplers with PEEK needle must have caps with slit septa • Never shake the vial. If you do there is going to be sample on the underside of the septum which gives carry over • Adjust the needle height according to the vial dimensions • Rubber septas get dry and can block the injector

The customer observed poor peak area precision, with relative standard deviations in the range of 1–2%. Troubleshooting the customer’s instrument, we found that the poor precision could be attributed to gas in the injection system. Gas bubbles in the injection system are a common issue with autosamplers.

Three sample-rack sizes are available for the autosamplers. The standard full-size rack holds 100 × 1.8 ml vials, while the two half-size racks provide space for 40 × 1.8 ml vials and 15 × 6 ml vials respectively. Any two half-size rack trays can be installed in the autosamplers simultaneously. A specially

Figure 1. Sample format and tray variety for the UltiMate 3000 WPS Autosamplers Series. Table 1. UltiMate 3000 Autosampler Sample Tray Formats Sample Containments Sample Tray*1 Total Vials in Carousel (plus 15 x 10 mL vials) Micro, cylindrical 0.3 mL vials 0.3 mL rack 3 × 72 = 216 Analytical, conical 1.1 mL vials 1.1 mL rack 3 × 40 = 120